3rd LAPRW Scientific Program


Sunday, May 8th, 2011

12.00 - 17.00 Registration Poster Hanging
17.30 - 18.00 OPENING CEREMONY

Sample Preparation & Mass Spectrometry applications for the Pesticide Residue Analysis in Foods: Actual and Future Trends
Chairpersons:
Stewart Reynolds and Horacio Beldomenico

18.30 - 18.30 O1 Validation of qualitative screening methods. Hans Mol
RIKILT Institute of Food Safety, The Netherlands
18.30 - 19.00 O2 Fast extraction and dilution flow injection mass spectrometry (FED-FI-MS): method design, applications, and outlook. Sergio Nanita.
DuPont Crop Protection, Stine-Haskell Research Center, U.S.A.
19.00 - 19.30 O3 State of the art techniques in mass spectrometry for pesticide residue analysis
Amadeo R. Fernández-Alba
University of Almeria, Spain
19.30 WELCOME COCKTAIL
 
Monday, May 9th,2011
Sample Preparation & Mass Spectrometry applications for the Pesticide Residue Analysis in Food
Chairpersons:
Amadeo R. Fernández-Alba and Tuija Pihlström
8.30 - 9.00 O4 Simplified analysis of pesticide residues in food using the swedish ethyl acetate method (SweEt).
Susanne Ekroth
National Food Administration, Science Department, Sweden
9.00 - 9.30 O5 Sample preparation and matrix effects in the detection of chemical residues in foods.
Steven Lehotay
US Department of Agriculture (USDA), USA
9.30 - 10.00 O6 Parameters affecting the extraction efficiency, clean-up efficiency and amount of co-extracted compounds in pesticide analysis of incurred pesticide residues in cereals.
Mette Erecius Poulsen
Technical University of Denmark, National Food Institute, Denmark
10.00 - 10.30 O7 Comparison of multi-residue methods to determine pesticide residues in fruit, vegetables and cereals by GC – Tandem Mass Spectrometry.
Vincent Hanot
Scientific Institute of Public Health, Belgium
10.30 - 11.00 Coffee break/Vendor Technical Seminar V1: Bruker Daltonics Inc.
Multiresidue pesticide screening by LC-ESI-TOF Mass Spectrometry
Grace Kelli Pereira
Bruker Daltonics, Brazil
  Chairpersons: André de Kok and Eloisa Dutra Caldas
11.00 - 11.30 O8 Development and validation of a UHPLC-ToFMS and UHPLC-MS/MS based approach for screening pesticide residues in fruit and vegetables.
Richard Fussell
Food and Environmental Research Agency, U.K.
11.30 - 12.00 O9 Pesticide residue analyses in food of animal origin.
Ralf Lippold
CVUA, Freiburg, Germany
12.00 - 12.30 O10 Basics of electrospray ionization
Lutz Alder
Federal Institute for Risk Assessment, Germany
12.30 - 14.00 Vendor Technical Seminar V2: AB Sciex
Target and non-target screening for pesticide residues in food samples using different LC-MS/MS techniques.
Enrique Servin
AB Sciex, México
  Chairpersons: Hans Mol and Ionara Pizzutti
14.00 - 14.20 O11 Chromatographic methods for the determination of pesticides residues in baby food
Maria Rosa Repetti
Central Laboratory, School of Chemical Engineering, UNL, Argentina
14.20 - 14.40 O12 Preparation of an incurred rice sample and evaluation of pesticide residues in the commodities obtained after processing.
Lucía Pareja
Cátedra de Farmacognosia y Productos Naturales, Facultad de Química, UdelaR, Uruguay
14.40 - 15.00 O13 Matrix effects in electrospray mass spectrometry - not a hopeless case.
Helen Stahnke
Federal Institute for Risk Assessment, Germany
15.00 - 15.20 Two Short Oral Presentations of Posters
15.30 - 16.00 Coffee break/ Vendor Technical Seminar V3: Gerstel GmbH
Automated QuEChERS extraction for the confirmation of pesticide residues in foods.
Alberto E. Aguilar-Sartori
Gerstel, Brasil
16.00 - 17.00 POSTERS SESSION
17.00 - 18.00 ROUND TABLE I: Sample preparation: Influence of MS detection techniques on sample preparation / extraction methods.
Amadeo R. Fernández-Alba, Richard Fussell, Ionara Pizzutti, André de Kok, Steven Lehotay, Vincent Hanot
Moderator: Hans Mol
18.00 - 19.00 Vendor Technical Seminar V4 : Restek
Comprehensive screening for PAHs in sugarcane products after QuEChERS with sweet separations using an Rxi-17Sil MS column, GC-MS, and GCxGC-TOFMS.
Julie Kowalski
Restek, USA
 
Tuesday, May 10th, 2011
Pesticide Regulation, Monitoring and Analysis
Chairpersons: Antonio Valverde and Susanne Ekroth
8.30 - 9.00 O14 The European (EU) coordinated multiannual control programme for pesticide residues in food.
Stewart Reynolds
Food and Environment Research Agency (FERA, UK)
9.00 - 9.30 O15 The U.S. food and drug administration’s pesticide monitoring and enforcement program.
Ronald R. Roy
Center for Food, Safety and Applied Nutrition, U
9.30 - 10.00 O16 INTI strategies for improving food quality and performance of pesticide residue laboratories in Argentina.
Patricia Gatti
National Institute of Industrial Technology (INTI), Argentina
10.00-10.30 O17 The national residue control plan in Brazil – policies and trends regarding to the laboratory activity.
Angelo Maurício de Queiroz
The Brazilian Ministry of Agriculture, Brazil
10.30 -11.00 Coffee break/ Vendor Technical Seminar V5: Bruker
Targeted and non-targeted screening of consumer products using nuclear magnetic resonance technique.
Sylvain Meguellatni
Bruker BioSpin GmbH, Germany

Chairpersons: Eduardo Dellacassa and Guy Jamet

11.00 - 11.30 O18 Pesticide residue analysis in Brazil: never too late
Adélia C.P. Araújo
Institute of Technology of Pernambuco, Brazil
11.30 - 12.00 019 Fast screening of more than 1000 pesticides and toxins using multiple analytical techniques at the US food and drug administration.
Chris A. Sack
Total Diet Research Center, US Food and Drug Administration, USA
12.00 - 12.30 020 Pesticide regulations in Uruguay.
Isabel Dol
Facultad de Química, UdelaR, Uruguay
12.30 - 14.00 Lunch
13.00 - 14.00 Vendor Technical Seminar V6 : Waters Corporation
Recent advances in mass spectrometry for pesticide residue analysis: quantitative ToF MS, atmospheric pressure GC, and ultra sensitive tandem quadrupole MS.
Kenneth J. Rosnack
Waters Corporation, U.S.A.

Quality Assurance / Quality control in Laboratorie performing Pesticide Residue Analysis (QA/QC)
Chairpersons: Lutz Alder and Patricia Pelos

14.00 - 14.20 O21 Method validation and analytical quality control procedures for pesticide residues analysis in the European Union.
Tuija Pihlström
National Food Administration, Science Department, Sweden
14.20 - 14.40 O22 Practical and valid approaches for realistic estimation of measurement uncertainty in multi-pesticide residue analysis.
Antonio Valverde
Pesticide Residue Research Group, University of Almeria, Spain
14.40 - 15.00 O23 Analytical quality control aspects achieved from EUPT-FV database.
Paula Medina
European Union Reference Laboratory for Pesticide Residues in Fruit and Vegetables. University of Almeria, Spain
15.00 - 15.20 Two Short Oral Presentations of Posters
15.30 - 16.00 Coffee break/ Vendor Technical Seminar V 7: LECO Corporation.
GC/TOFMS and GC×GC/TOFMS advances for pesticides analysis.
Carin von Mühlen
Pure and Technologycal Science Institute, Brazil
16.00 - 17.00 POSTERS SESSION
17.00 - 18.00 ROUND TABLE II QA/QC: Relevant topics for laboratories performing residue analysis in Latin America
Patricia Gatti, Chris Sack, Adélia C.P. Araújo, André de Kok, Antonio Valverde
Moderator: Stewart Reynolds
18.00 - 19.00 Vendor Technical Seminar V8 : UCT Inc.
The chemistry of solid phase extraction.
Michael J. Telepchak
UCT Inc., USA
 
Wednesday , May 11th, 2011
Dietary and Environmental Risk Assessment of Pesticides
Chairpersons: Ralf Lippold and Verónica Cesio
9.00 - 9.30 O24 Theory and methods of pesticide ecological risk.
Ronald Parker
Environmetal Fate and Effects Division, Office of Pesticide Programs, EPA, USA
9.30 - 10.00 O25 MELISSA: Investigations in the incidence of bee losses in corn and oilseed rape growing areas of Austria and possible correlations with bee diseases and the use of insecticidal plant protection products.
Sonja Masselter
Austrian Agency for Health and Food Safety GmbH, Austria
10.00 - 10.30 O26 Decreasing the impact of aflatoxin.
Ashli Brown
Mississippi State University, USA
10.30 - 11.00 Coffee break/ Vendor Technical Seminar V9: Bruker
Matrix matched standards reveal matrix MRM interferences and minimise false results in pesticide residue analysis of grains and pulses
Patrick Jeanville
Bruker Daltronics Inc., Fremont, CA
  Chairpersons: Silvia García and Sonja Masselter
11.00 - 11.30 O27 Microextraction of organic pollutants from liquid samples by using rotating-disk sorbent extraction.
Pablo Richter
Facultad Ciencias Químicas y Farmacéuticas, Universidad de Chile, Chile
11.30 - 12.00 O28 Maximum residues limits in Europe – the development and use of regulation 396/2005.
Caroline A. Harris
Center for Chemical Regulation and Food Safety, Exponent International Ltd, U.K.
12.00 - 12.30 O29 Pesticide residues in Brazilian food and the risks to human health.
Eloisa Dutra Caldas
Laboratory of Toxicology, University of Brasília, Brazil
12.30 - 14.00 Lunch
13.00 - 14.00 Vendor Technical Seminar V10 : Agilent Technologies
Pesticide residue analysis using advanced GC/MS/MS techniques.
Philip L. Wylie
Agilent Technologies, USA
Food safety by UHPLC/MS QqQ.
Juan Carlos López
Agilent Technologies, Mexico
  Chairpersons: Sergio Nanita and Richard Fussell
14.00 - 14.20 O30 Single SPE-Step method for the simultaneous determination of GC-MS and LC-MS amenable pesticides in water.
Zisis Vryzas
Democritus University of Thrace, Laboratory of Agricultural Pharmacology and Ecotoxicology, Greece.
14.20 - 14.40 O31 There is plenty of room for immunoassays, the Cinderella of the analytical tool menu.
Gualberto González-Sapienza
Facultad de Química, UdelaR, Uruguay
14.40 - 15.00 O32 Studies of pesticide residues in soil and water in the Lake Tota Catchment, Colombia
Jairo Guerrero Dallos
Laboratorio de Análisis de Residuos de Plaguicidas, Universidad Nacional de Colombia, Colombia.
15.00 - 15.20 Two Short Oral Presentations of Posters
15.30 - 16.00 O33 Speeding gas chromatography-Mass Spectrometry to analyze >150 pesticide residues in <10 min.
Steven Lehotay
US Department of Agriculture (USDA), USA
16.00 - 17.00 Posters awards.
Announcements of the IUPAC activities in the International Year of Chemistry
Announcements of next Pesticide Residue Workshops (LAPRW, EPRW, FPRW).
CLOSING CEREMONY